Publications OK SMART LAB

Demonstration of facile face-to-face assembly of cerium oxide-coated carbon nanotube forest blocks for room-temperature-operable, high-surface-area gas sensing system
Authors
Jaehyeok Yang, Minwook Kim, Jinkyu Han, Yeongjun Heo, Kwangjun Kim, Jongwon Park, Taeyun Kim, Kyungho Lee, Jong G. Ok
Journal
한국기계가공학회지 (Journal of the Korean Society of Manufacturing Process Engineers)
Vol. (No.), pp. (Year)
24(12), 9-17 (Dec 2025)
Category
A facile, lithography-free fabrication strategy based on the face-to-face (F2F) assembly of carbon nanotube (CNT) forest blocks conformally coated with cerium dioxide (CeO₂) is demonstrated for a gas sensor operable at room temperature. A thermally stable TiN base electrode provides an electrically conductive and heat-resistant foundation during the atmospheric CVD growth of vertically aligned CNT forests on an Fe catalyst layer, while the CeO₂ coating introduces an n-type semiconductor interface that forms a p–n junction with the p-type CNT network. Through simple F2F assembly of the two blocks, three device types (CNT + CNT blocks, CeO₂/CNT + CeO₂/CNT blocks, and CNT + CeO₂/CNT blocks) are fabricated and systematically compared to elucidate the sensing mechanism and optimize the configuration. Among them, the asymmetric CNT + CeO₂/CNT device exhibits the most stable and sensitive response, reliably detecting NO₂ concentrations as low as 10 ppm even at room temperature and reaching a sensitivity of approximately 6.2 % at 120 °C for 30 ppm NO2. The superior sensing behavior arises from efficient charge transfer across the CeO₂/CNT interface and favorable adsorption-desorption kinetics provided by the high surface area of the CNT forest. These results verify the feasibility of compact, low-power NOx detection using a hybrid CeO₂/CNT structure for industrial and automotive sensing applications.